[유기화학실험 A+] Diels-Alder Reaction (1,3-Butadiene) (prelab/프리랩/예비보고서)
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"[유기화학실험 A+] Diels-Alder Reaction (1,3-Butadiene) (prelab/프리랩/예비보고서)"에 대한 내용입니다.
목차
1. Objectives
2. Principles & Methods
3. References
본문내용
Objectives: Diels-Alder reaction of (E,E)-2,4-hexadien-1-ol and maleic anhydride can be carried out to synthesize (3aR,4S,5S,7aR)-5-methyl-3-oxo-1,3,3a,4,5,7a-hexahydroisobenzofuran-4-carboxylic acid.
Principles & Methods
(1) Principles: Diels-Alder Reaction is a cycloaddition between a 1,3-diene and an electron-poor alkene (= dienophile) to provide in a single step a cyclohexene derivative.
참고 자료
John A. Landgrebe. “Theory and Practice in the Organic Laboratory” 5th ed. 2005. Thomson Wadsworth.
Leory G. and Jan William Simek. “Organic Chemistry” 2017 Pearson.
McDaniel, K. F., & Weekly, R. M. (1997). The Diels-Alder Reaction of 2,4-Hexadien-1-ol with Maleic Anhydride: A Novel Preparation for the Undergraduate Organic Chemistry Laboratory Course. Journal of Chemical Education, 74(12), 1465. doi:10.1021/ed074p1465
https://chem.libretexts.org/Bookshelves/Organic_Chemistry/Organic_Chemistry_Lab_Techniques_(Nichols)/02%3A_Chromatography/2.03%3A_Thin_Layer_Chromatography_(TLC)/2.3F%3A_Visualizing_TLC_Plates
https://chem.libretexts.org/Bookshelves/Organic_Chemistry/Map%3A_Organic_Chemistry_(Wade)/16%3A_Conjugated_Systems_Orbital_Symmetry_and_Ultraviolet_Spectroscopy/16.06%3A_The_Diels-Alder_(4__2)_Cycloaddition_Reaction
https://www.sciencedirect.com/topics/biochemistry-genetics-and-molecular-biology/lactonization
Wikipedia (“Diels-Alder reaction”, “Lactone”, “Enantiomer”)
https://pubchem.ncbi.nlm.nih.gov
chemspider.com