Synthesis of Nitrobenzene(니트로벤젠 합성 실험) 예비/결과 레포트
- 최초 등록일
- 2024.06.25
- 최종 저작일
- 2023.05
- 16페이지/
MS 워드
- 가격 2,500원
소개글
성균관대학교, Synthesis of Nitrobenzene 니트로벤젠 합성 실험의 예비/결과 레포트입니다. 레포트 두개 분량이다 보니 정보가 많습니다. 본 과목 A+ 성적으로 이수했습니다.
목차
1. Title
2. Objective
3. Theoretical Background
4. Apparatus & Reagent
5. Experimental Procedure
6. Pre-Lab report
7. Reference
1. Result
2. Discussion
3. Report
4. Summary
5. Reference
본문내용
1. Title: Synthesis of Nitrobenzene
2. Objective
-to synthesize nitrobenzene using nitric acid and sulfuric acid as reactants
-to experience basic operations which are going to be used.
3. Theoretical Background
1) Property of Nitrobenzene
Nitrobenzene (C6H5NO2) is an organic aromatic nitro compound. Nitrobenzene is highly toxic and can be ingested, inhaled or absorbed through the skin. Therefore, care must be taken in handling the experimental. Also, nitrobenzene does not dissolve well in water, which can be confirmed during the experiment. Nitrobenzene has a molecular weight of 123 g/mol. It has a melting point of 5.8℃, a boiling point of 211℃, and a specific gravity of 1.2, and exists as a colorless liquid at room temperature. Benzene also acts as a base that can give electrons in a reaction. So it reacts easily to the pro-electrolyte and acid.
참고 자료
[Experimental procedure] “Chemical Engineering Laboratory I”, Sungkyunkwan University School of Chemical Engineering
https://safety.skku.edu/ - MSDS
Cai Y, Hua Y, Lu Z, Lan Q, Lin Z, Fei J, Chen Z, Zhang H, Xia H. Electrophilic aromatic substitution reactions of compounds with Craig-Möbius aromaticity. Proc Natl Acad Sci U S A. 2021 Sep 28;118(39):e2102310118. doi: 10.1073/pnas.2102310118. PMID: 34544859; PMCID: PMC8488665.
Surkau J, Bläsing K, Bresien J, Michalik D, Villinger A, Schulz A. A Lewis Acid Stabilized Ketenimine in an Unusual Variant of the Electrophilic Aromatic Substitution. Chemistry. 2022 Dec 1;28(67):e202201905. doi: 10.1002/chem.202201905. Epub 2022 Oct 7. PMID: 35989474; PMCID: PMC10092272.
Jae Seung Oh, Sang Moo Lee, Jong Kee Yeo, Chul Woo Lee, and Jae Sung Lee. Palladium-catalyzed synthesis of N,N'-diphenylurea from nitrobenzene, aniline, and carbon monoxide. Industrial & Engineering Chemistry Research 1991 30 (7), 1456-1461. DOI: 10.1021/ie00055a009
